Analysis of microstress in neutron irradiated polyester fibre by X-ray diffraction technique |
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Authors: | B Mallick R C Behera T Patel |
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Affiliation: | (1) Institute of Physics, Sachivalay Marg, 751 005 Bhubaneswar, India;(2) Department of Metallurgical and Materials Engineering, National Institute of Technology, 769 008 Rourkela, India;(3) Department of Physics, National Institute of Technology, 769 008 Rourkela, India |
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Abstract: | Microstresses developed in the crystallites of polymeric material due to irradiation of high-energy particle causes peak broadening
and shifting of X-ray diffraction lines to lower angle. Neutron irradiation significantly changes the material properties
by displacement of lattice atoms and the generation of helium and hydrogen by nuclear transmutation. Another important aspect
of neutron irradiation is that the fast neutron can produce dense ionization at deep levels in the materials. The polyethylene
terephthalate (PET) fibre of raw denier value, 78.2, were irradiated by fast neutron of energy, 4.44 MeV, at different fluences
ranging from 1×109 n/cm2 to 1 × 1012 n/cm2. In the present work, the radiation heating microstresses developed in PET micro-crystallites was investigated applying X’Pert-MPD
Philips Analytical X-ray diffractometer and the effects of microstresses in tensile strength of fibre measured by Instron
have also been reported. The shift of 0.45 cm−1 in the Raman peak position of 1614.65 cm{−1} to a higher value confirmed the development of microstresses due to neutron irradiation using micro-Raman technique. The
defects due to irradiation were observed by SEM micrographs of single fibre for virgin and all irradiated samples. |
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Keywords: | Microstress PET neutron fluences XRD SEM micro-Raman technique |
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