Synthesis of PDMS-PS IPN Pervaporation Membrane for Pervaporation Recovery of Butanol |
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Authors: | Wei Yu Xiaoquan Sun Ziye Wu Li Sun Mingjie Hu Houbin Li Chi Huang |
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Affiliation: | 1.College of Chemistry and Molecular Sciences,Wuhan University,Wuhan,China;2.Hubei Military-Civilian Integration and Co-Innovation Center of Aerospace Power and Materials Technology,Wuhan,China;3.Luzhou North Chemical Industres Co.,Ltd,Luzhou,China;4.School of Printing and Packaging,Wuhan University,Wuhan,China |
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Abstract: | Polydimethylsiloxane (PDMS)-polystyrene (PS) interpenetrating polymer network (IPN) was prepared and characterized by FTIR, TGA, WCA, swelling experiments, and SEM. The IPN was used for pervaporation (PV) recovery of butanol. Both the permeation flux and separation factor increased with feed temperature, and both water and butanol fluxes increased with feed concentration, while no obvious effect of concentration on separation factor was found. Through the formation of IPN structure, the total flux of PDMS-PS IPN pervaporation membrane increased greatly with the decrease of separation factor. At the feed temperature of 60 °C, the IPN membrane obtained a total flux of 920.3 g/m2h with a separation factor of 9.5. |
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