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硫脲对喷射电铸纳米晶铜组织与性能的影响
引用本文:赵阳培,葛世荣,张君伟,黄因慧. 硫脲对喷射电铸纳米晶铜组织与性能的影响[J]. 金属热处理, 2009, 34(2): 40-43
作者姓名:赵阳培  葛世荣  张君伟  黄因慧
作者单位:中国矿业大学,材料与工程学院,江苏,徐州,221008;徐州建筑职业技术学院,江苏,徐州,221008;中国矿业大学,材料与工程学院,江苏,徐州,221008;徐州建筑职业技术学院,江苏,徐州,221008;南京航空航天大学,机电学院,江苏,南京,210016
摘    要:采用喷射电铸法制备了不同硫脲浓度下的纳米晶铜铸层,用SEM、XRD方法分析了硫脲对纳米晶铜铸层微观结构和晶粒大小的影响,并对纳米晶铜铸层的力学性能进行了测试.结果表明,硫脲能细化晶粒,致密铸层组织,显著提高铸层的抗拉强度和显微硬度;电铸液中硫脲浓度为10 mg/L时,可获得晶粒尺寸为29 nm的致密铜铸层,其显微硬度和抗拉强度分别为3.1 GPa和645 MPa.电铸液中硫脲浓度从5 mg/L增至10 mg/L时,纳米晶铜铸层的择优取向由(220)晶面转变为(111)晶面.

关 键 词:硫脲  纳米晶铜  微观组织  力学性能

Effects of thiourea on microstructure and properties of nanocrystalline copper prepared by jet electroforming
ZHAO Yang-pei,GE Shi-rong,ZHANG Jun-wei,HUANG Yin-hui. Effects of thiourea on microstructure and properties of nanocrystalline copper prepared by jet electroforming[J]. Heat Treatment of Metals, 2009, 34(2): 40-43
Authors:ZHAO Yang-pei  GE Shi-rong  ZHANG Jun-wei  HUANG Yin-hui
Affiliation:1.Material Science and Engineering College;China University of Mining and Technology;Xuzhou Jiangsu 221008;China;2.Xuzhou Institute of Architectural Technology;3.College of Mechanical and Electrical Engineering;Nanjing University of Aeronautics and Astronautics;Nanjing Jiangsu 210016;China
Abstract:Nanocrystalline copper was fabricated by jet electroforming with different concentration of thiourea.The microstructure and grain sizes of the copper deposits were studied by means of SEM and XRD,and the mechanical properties of nanocrystalline copper were measured.The results show that the fine grain and dense deposits with high tensile strength and microhardness can be got by adding thiourea to the electrolyte,the dense nanocrystalline copper deposit with average grain size of 29 nm is fabricated with the...
Keywords:thiourea  nanocrystalline copper  microstructure  mechanical properties  
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