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Survey of the anticoccidial feed additive nicarbazin (as dinitrocarbanilide residues) in poultry and eggs
Authors:Martin Danaher  Katrina Campbell  Michael O’Keeffe  Emiliana Capurro  Glenn Kennedy  Christopher T. Elliott
Affiliation:1. Food Safety Department , Ashtown Food Research Centre , Teagasc, Dunsinea, Ashtown, Dublin 15, Ireland martin.danaher@teagasc.ie;3. Institute of Agri-Food and Land Use, Queen's University Belfast , David Keir Building, Stranmillis Road, Belfast BT9 5AG, UK;4. Food Safety Department , Ashtown Food Research Centre , Teagasc, Dunsinea, Ashtown, Dublin 15, Ireland;5. Agri-Food and Biosciences Institute , Stoney Road, Stormont, Belfast, BT4 3SD, UK
Abstract:A survey was carried out on the occurrence of dinitrocarbanilide (DNC), the marker residue for nicarbazin, in poultry produced in Ireland during 2002–2004. Liver (n?=?736) and breast muscle samples (n?=?342) were tested. DNC residues were found in 40 and 26% of liver and breast muscle samples at levels greater than 12.5 and 5?µg?kg?1, respectively. DNC residues were found at >200?µg?kg?1 in 12 and 0% of liver and muscle samples, respectively. Samples of breast muscle (n?=?217) imported from 11 countries were also tested for DNC residues. A lower incidence of DNC residues (6%) was found in imported breast muscle. Egg samples (n?=?546) were tested and DNC residues were found in nine samples, with levels ranging between 14 and 122?µg?kg?1. Analysis of poultry, carried out as part of official food inspection in the period 2004–2006, indicated a reduction in the number of broiler liver samples containing DNC at >200?µg?kg?1, to approximately 7%. Low levels of DNC residues continue to be found in <2% of egg samples.
Keywords:HPLC  LC/MS  screening  biosensor  survey  residues  animal products  meat  eggs
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