| 硼酸三甲酯无“三废”合成工艺 |
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| 引用本文： | 刘道明,周章凯,杨成. 硼酸三甲酯无“三废”合成工艺[J]. 河北化工, 2011, 34(9): 18-19,38 |
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| 作者姓名： | 刘道明 周章凯 杨成 |
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| 作者单位： | 安徽金邦医药化工有限公司,安徽怀远,239200 |
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| 摘 要： | 以硼酸、甲醇为原料,用甲酰胺对产物进行萃取提纯,合成硼酸三甲酯,探索了最佳工艺条件。利用气相色谱、色谱-质谱联用、红外光谱等分析表征手段,鉴定反应产物,最佳工艺条件：n硼酸：n甲醇=1∶3.5;回流时间为4 h。此工艺无＂三废＂排放,有利于工业化生产。
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| 关 键 词： | 硼酸 甲醇 甲酰胺 硼酸三甲酯 萃取 |
Synthesis Process of Trimethyl borate |
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| LIU Dao-ming,ZHOU Zhang-kai,YANG Cheng. Synthesis Process of Trimethyl borate[J]. Hebei Chemical Engineering and Industry, 2011, 34(9): 18-19,38 |
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| Authors: | LIU Dao-ming ZHOU Zhang-kai YANG Cheng |
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| Affiliation: | LIU Dao-ming,ZHOU Zhang-kai,YANG Cheng(Anhui Jinbang Medicine Chemical Co.,Ltd,Huaiyuan 239200,China) |
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| Abstract: | Trimethyl borate was synthesized as raw material with boric acid and methly alcohol and formamide as extrac-tive,and the optimum condition was chosen by experiments.By means of gas chromatography,mass spectrometry and IR spectrum,the product was confirmed.The optimum conditions were that n（acid）∶n（alcohol）=1∶3.5 for 4 h This craft which has no＂three wastes＂the emissions is advantageous in the industrialization production. |
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| Keywords: | boric acid methly alcohol formamide trimethyl borate extractivation |
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