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An Efficient and Facile Synthesis of CL‐20 from TADNO Using HNO3/N2O5 and Optimization of Reaction Parameters by Taguchi Method
Authors:Yadollah Bayat  Fatemeh Hajighasemali
Abstract:Hexanitrohexaazaisowurtzitane (CL‐20) is an outstanding member of a promising new class of energetic compounds, which is applicable in both propellants and explosives. Herein, CL‐20 was synthesized in an efficient method from tetraacetyldinitrosohexaazaisowurtzitane (TADNO) using N2O5/HNO3. The optimization reaction parameters were performed according to the Taguchi OA method. The yield of reaction at the optimized conditions was 97 % with 98.75 % purity.
Keywords:TADNO  CL-20  Dinitrogen Pentoxide  Qualitek-4  Taguchi OA
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