| 聚苯胺/镍纳米复合材料的制备及其表征 |
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| 引用本文： | 杨艳华,罗驹华,郑锐林,朱双美.聚苯胺/镍纳米复合材料的制备及其表征[J].化工进展,2009,28(9):1623. |
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| 作者姓名： | 杨艳华 罗驹华 郑锐林 朱双美 |
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| 作者单位： | 南京工业大学材料科学与工程学院；盐城工学院江苏省生态环境材料重点建设实验室；河南工程学院 |
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| 基金项目： | 江苏省无机及其复合新材料重点实验室资助项目(wjjqfhxc1200504);;江苏省高等学校大学生实践创新训练计划项目(200804) |
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| 摘 要： | 以苯胺（An）、氯化镍（NiCl2×6H2O）为原料，原位聚合法合成聚苯胺/镍纳米复合微粒。采用X射线衍射仪、扫描电镜、傅里叶变换红外光谱仪、振动样品磁强计（VSM）及四探针测试仪技术表征了复合微粒的结构、形貌和电磁性能。结果表明：复合微粒在室温外加磁场下表现出铁磁性物质具有的磁滞现象，饱和磁化强度为9.44 emu/g，复合微粒在室温下的电导率为5×10-3 S/cm。
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| 关 键 词： | 镍 聚苯胺 纳米复合材料 磁性 电导率 |
Preparation and characterization of polyaniline/nickel nanocomposites |
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| YANG Yanhua,LUO Juhua,ZHENG Ruilin,ZHU Shuangmei.Preparation and characterization of polyaniline/nickel nanocomposites[J].Chemical Industry and Engineering Progress,2009,28(9):1623. |
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| Authors: | YANG Yanhua LUO Juhua ZHENG Ruilin ZHU Shuangmei |
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| Affiliation: | College of Materials Science and Engineering，Nanjing University of Technology；Jiangsu Provincial Key Laboratory of Eco-environmental Materials，Yancheng Institute of Technology；Henan University of Engineering |
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| Abstract: | Polyaniline-Ni nanocomposites were synthesized by in situ aqueous polymerization of aniline in the presence of Ni. The structure、norphologies、magnetic and electrical properties of samples were characterized by scanning electron microscope (SEM)，X-ray diffraction(XRD)，Fourier transform infrared spectra (FTIR)，four probe method and vibrating sample magnetometer(VSM) techniques.The results indicated that the nanocomposites under applied magnetic field exihibited the hysteresis loops of the ferromagnetic nature at room temperature，Saturation magnetization was 9.44 emu/g. The electrical conductivity was 5×10-3 S/cm. |
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| Keywords: | nickel polyaniline nanocomposites magnetic properties conductivity |
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