Synthesis of chemically coprecipitated hexagonal strontium-ferrite and its characterization |
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Authors: | Shailaja Kulkarni Jyotsna Shrotri C. E. Deshpande S. K. Date |
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Affiliation: | (1) Physical Chemistry Division, National Chemical Laboratory, 008 Pune-411, India |
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Abstract: | Highly uniform submicrometre size particles of hexagonal strontium ferrite (SrFe12O19) have been synthesized by chemical coprecipitation technique at pH ⋍ 13. Chemical coprecipitation technique has helped in bringing down the ferritization temperature from 1300 to 925° C which is revealed by DTA-TG and XRD studies. Reproducible uniform single domain particle size and its distribution has been observed by scanning electron microscopy. X-ray and Mossbauer studies have identified single phase ferrite with Fe3+ ions occupying the proper crystallographic sites. The performance parameters of the sintered isotropic strontium ferrite magnets have proved to be superior by about 20% over the ferrites prepared by conventional ceramic technique. |
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