| 对氯间二甲酚合成新工艺 |
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| 引用本文： | 魏文珑,田向农,常红红. 对氯间二甲酚合成新工艺[J]. 应用化工, 2006, 35(2): 99-100,103 |
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| 作者姓名： | 魏文珑 田向农 常红红 |
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| 作者单位： | 太原理工大学,化学与化工学院,山西,太原,030024 |
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| 摘 要： | 以间二甲酚和氯气为原料,在三氯化铝的催化下合成了对氯间二甲酚,最佳工艺条件为:四氯化碳70 mL,60℃下通氯反应90 m in,收率可以达61.1%。
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| 关 键 词： | 间二甲酚 氯化 对氯间二甲酚 三氯化铝 |
| 文章编号： | 1671-3206（2006）02-0099-02 |
| 收稿时间： | 2005-11-25 |
| 修稿时间： | 2005-11-25 |
New technics for synthesis of chloroxylenol |
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| WEI Wen-long,TIAN Xiang-nong,CHANG Hong-hong. New technics for synthesis of chloroxylenol[J]. Applied chemical industry, 2006, 35(2): 99-100,103 |
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| Authors: | WEI Wen-long TIAN Xiang-nong CHANG Hong-hong |
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| Affiliation: | College of Chemistry and Chemical Engineering, Taiyuan University of Technology,Taiyuan 030024, China |
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| Abstract: | Chloroxylenol was prepared from 3,5-xylenol and chlorine by using aluminum chloride as catalyst.The optimum synthetic conditions were found as follows:carbon tetrachloride is 70 mL,reaction time is 90 min,reaction temperature is 60℃,the chloroxylenol yield may reach 61.1%. |
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| Keywords: | 3,5-xylenol chlorination chloroxylenol aluminum chloride |
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