| 茶叶中锗、硒的电感耦合等离子体质谱法分析 |
| |
| 引用本文： | 侯冬岩,回瑞华,李红,刘俊会,华蕾.茶叶中锗、硒的电感耦合等离子体质谱法分析[J].质谱学报,2008,29(6):353-355. |
| |
| 作者姓名： | 侯冬岩 回瑞华 李红 刘俊会 华蕾 |
| |
| 作者单位： | 1. 鞍山师范学院，辽宁 鞍山 114007；
2.国家农业深加工产品质量监督检验中心, 吉林 长春 130002 |
| |
| 摘 要： | 采用微波消解,电感耦合等离子体质谱(ICP-MS)法测定茶叶中锗、硒元素。对样品前处理方法进行了研究，从消解体系、酸用量、消解程序等方面对微波消解条件进行了优化。在优化实验条件下, 方法的检出限为1.7~28.2 ng?L-1, 相对标准偏差为3.1%~10.0%, 加标回收率为80.8%～95.9%。该方法具有操作简便，快速，灵敏度高，准确度好和同时测定两种元素等优点。
|
| 关 键 词： | 电感耦合等离子体-质谱法 微波消解 茶叶 锗 硒 |
| 收稿时间： | 2008-04-03 |
Determination of Germanium and Selenium in Teas by ICP-MS |
| |
| HOU Dong-yan,HUI Rui-hua,LI Hong,LIU Jun-hui,HUA Lei.Determination of Germanium and Selenium in Teas by ICP-MS[J].Journal of Chinese Mass Spectrometry Society,2008,29(6):353-355. |
| |
| Authors: | HOU Dong-yan HUI Rui-hua LI Hong LIU Jun-hui HUA Lei |
| |
| Affiliation: | 1.Department of Chemistry, Anshan Normal University, Anshan 114007，China;
2. China Quality Supervision & Testing Center for Agricultural Deep Processing Products, Changchun 130002, China
|
| |
| Abstract: | Germanium and selenium in teas were mensurated by ICP-MS. A digestion method was established for germanium and selenium in teas. The microwave digestion condition was optimized from digestion system, proportion of acids and digestion procedure. The detection limit is in the range of 1.7-28.2 ng?L-1, with the relative standard deviations of 3.1%-10.0%, and the recoveries are 80.8%-95.9%. The method is simple, rapid and reliable. |
| |
| Keywords: | ICP-MS microwavedigestion teas germanium selenium |
| 本文献已被 维普 万方数据 等数据库收录！ |
| 点击此处可从《质谱学报》浏览原始摘要信息 |
|
点击此处可从《质谱学报》下载全文 |
|
