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Observation of micro-cavities in nickel during He and D irradiation and post-irradiation annealing |
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| Authors: | K Niwase T Ezawa T Tanabe and F E Fujita |
| Affiliation: | a Department of Physics, Hyogo University of Education, Yashiro, Hyogo 673-14, Japan b Department of Material Physics, Faculty of Engineering Science, Osaka University, Toyonaka, Osaka 560, Japan c Department of Nuclear Engineering, Faculty of Engineering, Osaka University, Suita, Osaka 565, Japan |
| Abstract: | Changes in sizes and morphology of small cavities in nickel irradiated by 25 keV helium ions and 20 keV deuterons were investigated during irradiation and on annealing after irradiation by means of transmission electron microscopy. In the early stage of He+ irradiations at 600 and 700° C, roundish cubes appeared, gradually changed to octahedra. and, then, by the truncation of apexes, finally reached cubo-octahedra. Nucleation and growth behavior of cubic cavities in D+ irradiated nickel was different from the case of He+ irradiation. On annealing of the He+ irradiated specimen, only octahedral cavities showed marked growth, finally changing to roundish cubes at 750° C. Cavities of roundish cubes and cubo-octahedra did not grow nor change their shapes remarkably by the annealing. The cubic cavities formed by D+ irradiation at 360° C showed gradual shrinkage on annealing at 600° C and disappeared at 625° C. The changes of cavities during irradiation and on annealing were interpreted by the effect of the internal gas pressure. |
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