| 4,4,4-三苯基-1-丁烯-3-酮的合成研究 |
| |
| 引用本文： | 刘虎,阳年发,廖高荣. 4,4,4-三苯基-1-丁烯-3-酮的合成研究[J]. 化学试剂, 2011, 33(3): 274-276 |
| |
| 作者姓名： | 刘虎 阳年发 廖高荣 |
| |
| 作者单位： | 湘潭大学,化学学院,环境友好化学与应用教育部重点实验室,湖南,湘潭,411105 |
| |
| 基金项目： | 国家自然科学基金资助项日,湖南省自然科学基金资助项日 |
| |
| 摘 要： | 从三苯甲烷出发经过甲酰化,再与乙烯基溴化镁加成.氧化,高收率的合成了标题化合物.同时,对各步反应的实验条件进行了优化,找到了较好的合成条件,并用1HNMR和13CNMR对各步产物进行了表征.
|
| 关 键 词： | 4,4,4-三苯基-1-丁烯-3-酮 合成 大基团 |
Synthesis of 4,4,4-triphenyl-1-butlene-3-one |
| |
| LIU Hu,YANG Nian-fa,LIAO Gao-rong. Synthesis of 4,4,4-triphenyl-1-butlene-3-one[J]. Chemical Reagents, 2011, 33(3): 274-276 |
| |
| Authors: | LIU Hu YANG Nian-fa LIAO Gao-rong |
| |
| Affiliation: | LIU Hu,YANG Nian-fa,LIAO Gao-rong(Key Laboratory of Environment-Friendly Chemistry and Applications of Ministry of Education,College of Chemistry,Xiangtan University,Xiangtan 411105,China) |
| |
| Abstract: | 4,4,4-Triphenyl-1-butlene-3-one was synthesized from triphenylmethane via formulation,addition reaction and oxidation.The suitable reaction conditions were obtained and structures of the products were identified by 1HNMR and 13CNMR. |
| |
| Keywords: | 4 4-triphenyl-1-butlene-3-one synthesis bulky group |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
