| 超声萃取/ 快速溶剂萃取-气质联用测定烟用拉线中邻苯二甲酸酯类物质 |
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| 引用本文： | 刘丹,程娟,方细玲,邝淑婷,王志伟. 超声萃取/ 快速溶剂萃取-气质联用测定烟用拉线中邻苯二甲酸酯类物质[J]. 包装工程, 2013, 34(19): 14-17,23 |
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| 作者姓名： | 刘丹 程娟 方细玲 邝淑婷 王志伟 |
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| 作者单位： | 广东中烟工业有限责任公司技术中心, 广州510385,1. 广东省普通高校产品包装与物流重点实验室, 暨南大学, 珠海519070; 2. 暨南大学包装工程研究所, 珠海519070,广东中烟工业有限责任公司技术中心, 广州510385,1. 广东省普通高校产品包装与物流重点实验室, 暨南大学, 珠海519070; 2. 暨南大学包装工程研究所, 珠海519070,1. 广东省普通高校产品包装与物流重点实验室, 暨南大学, 珠海519070; 2. 暨南大学包装工程研究所, 珠海519070 |
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| 基金项目： | 国家自然科学基金项目资助(21277061, 21077045) |
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| 摘 要： | 建立了采用气相色谱-质谱联用法(GC-MS) 同时检测10 种邻苯二甲酸酯类物质的方法,并用此方法测出了5 种烟用拉线中含有的2 种邻苯二甲酸酯类物质DEHP 和DIBP 的含量。以正己烷为提取溶剂,分别采用超声提取法和ASE 快速溶剂萃取法对烟用拉线进行了萃取。结果表明,超声提取的回收率在78. 3% ~91. 7%之间,RSD 在7. 95% ~9. 82%之间,ASE 萃取技术的回收率在82. 2% ~93. 8%之间,RSD 在4. 95% ~7. 87%之间;ASE 萃取技术有较高的回收率和精密度,适宜用于烟用拉线检测前的处理过程。
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| 关 键 词： | 烟包拉线 邻苯二甲酸酯 超声萃取 快速溶剂萃取 气相色谱-质谱法 |
| 收稿时间： | 2013-02-20 |
| 修稿时间： | 2013-10-10 |
Determination of Phthalates in Tear Tapes for Cigarette Packaging Using Ultrasonic Extraction / ASE Method Coupling with GC-MS |
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| LIU Dan,CHENG Juan,FANG Xi-ling,KUANG Shu-ting and WANG Zhi-wei. Determination of Phthalates in Tear Tapes for Cigarette Packaging Using Ultrasonic Extraction / ASE Method Coupling with GC-MS[J]. Packaging Engineering, 2013, 34(19): 14-17,23 |
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| Authors: | LIU Dan CHENG Juan FANG Xi-ling KUANG Shu-ting WANG Zhi-wei |
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| Affiliation: | China Tobacco Guangdong Industrial Co. , Ltd. , Guangzhou 510385, China,1. Key Laboratory of Product Packaging and Logistics of Guangdong Higher Education Institutes, Jinan University, Zhuhai 519070, China; 2. Packaging Engineering Institute, Jinan University, Zhuhai 519070, China,China Tobacco Guangdong Industrial Co. , Ltd. , Guangzhou 510385, China,1. Key Laboratory of Product Packaging and Logistics of Guangdong Higher Education Institutes, Jinan University, Zhuhai 519070, China; 2. Packaging Engineering Institute, Jinan University, Zhuhai 519070, China and 1. Key Laboratory of Product Packaging and Logistics of Guangdong Higher Education Institutes, Jinan University, Zhuhai 519070, China; 2. Packaging Engineering Institute, Jinan University, Zhuhai 519070, China |
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| Abstract: | A GC-MS method for simultaneous detection of 10 kinds of phthalates was developed. DEHP and DIBP were detected in 5 kinds of tear tapes for cigarette packaging, and the contents were determined using the method. The phthalates was extracted with hexane by ultrasonically assisted procedure and ASE method respectively. The recoveries of the phthalates are between 70. 8% ~91. 7% with relative standard deviations of 7. 95% ~9. 82% when dealing with the ultrasonically assisted procedure, and between 82. 2% ~ 93. 8%% with relative standard deviations of 4. 95% ~ 7. 87% by the ASE procedure. It was concluded that the ASE procedure is the better pretreatment of tear tape for cigarette packaging. |
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| Keywords: | tear tape for cigarette packaging phthalates ultrasonic extraction ASE GC-MS |
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