| N-长链胆酸酰胺的合成 |
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| 引用本文： | 王立中,卞小琴,周兰香,李双双,李广州,王存德.N-长链胆酸酰胺的合成[J].化学工程师,2012(7):8-10,72. |
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| 作者姓名： | 王立中 卞小琴 周兰香 李双双 李广州 王存德 |
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| 作者单位： | 1. 泰州职业技术学院环境与化学工程系,江苏泰州,225300
2. 扬州大学化学化工学院,江苏扬州,225002 |
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| 基金项目： | 江苏省高等学校大学生实践创新训练计划项目，江苏青蓝工程项目和泰州职业技术学院科研项目 |
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| 摘 要： | 本文研究了具有长脂链胆酸基非离子型表面活性剂的合成,以商品化胆酸和一系列的长链伯胺(C12~C18)为原料,经过多步反应获得了N-长链烷基胆酸酰胺。目标化合物结构经IR,1H-NMR,13C-NMR,LC-MS等表征确证,同时,对其表面活性进行了初步研究。
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| 关 键 词： | 三甲酰氧基胆酸酰氯 三甲酰氧基胆酸酰胺 胆酸酰胺 合成 |
Synthesis of N-long-chain alkyl cholic amide |
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| WANG Li-zhong
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BIAN Xiao-qin
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ZHOU Lan-xiang
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LI Shuang-shuang
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Li Guang-zhou
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WANG Cun-de.Synthesis of N-long-chain alkyl cholic amide[J].Chemical Engineer,2012(7):8-10,72. |
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| Authors: | WANG Li-zhong BIAN Xiao-qin ZHOU Lan-xiang LI Shuang-shuang Li Guang-zhou WANG Cun-de |
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| Affiliation: | 1 .Department of Environmental and Chemical Engineering, Taizhou Polytechnic College, Taizhou 225300, China; 2.Sehool of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002,China) |
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| Abstract: | The long-chain alkyl cholic amide derivatives were synthesized using bile acid and long-chain alkyl amines as starting materials. All these structures were confirmed by IR, ^1H-NMR,^13C-NMR,LC-MS and their tensionmetrie property was tested. The results were indicated that the long-chain alkyl induced in the cholic acid increased its hydrophobic property. |
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| Keywords: | trimethanoyl cholic acid chloride trimethanoyl cholic acylamide cholic acylamide synthesis |
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