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多孔玻璃粉的制备及其在玻璃基板上的粘接
引用本文:任媛媛,韩建军,毛雨,袁启华,赵修建.多孔玻璃粉的制备及其在玻璃基板上的粘接[J].材料科学与工程学报,2012,30(1):89-92,127.
作者姓名:任媛媛  韩建军  毛雨  袁启华  赵修建
作者单位:武汉理工大学硅酸盐建筑材料国家重点实验室,湖北武汉,430070
基金项目:新世纪优秀人才支持计划资助项目,973计划前期研究专项资助项目
摘    要:利用硼硅酸盐玻璃的分相和酸侵蚀制备了孔径可控的多孔玻璃粉,采用SEM、BET等测试手段对玻璃的表面形貌和孔径分布进行了表征。并以Na2O-Al2O3-B2O3体系低熔点玻璃作为粘接剂将多孔玻璃粉烧结在普通玻璃板上,研制出一种表面孔径约50nm且均匀分布的多孔玻璃基板,并分析了烧结温度、烧结时间、颗粒大小等对粘接的影响。

关 键 词:多孔玻璃粉  热处理条件  低熔点玻璃  粘接

Preparation of Porous Glass Powder and its Adhesion with Glass Substrate
REN Yuan-yuan,HAN Jian-jun,MAO Yu,YUAN Qi-hua,ZHAO Xiu-jian.Preparation of Porous Glass Powder and its Adhesion with Glass Substrate[J].Journal of Materials Science and Engineering,2012,30(1):89-92,127.
Authors:REN Yuan-yuan  HAN Jian-jun  MAO Yu  YUAN Qi-hua  ZHAO Xiu-jian
Affiliation:(State Key Laboratory of Silicate Materials for Architectures(Wuhan University of Technology),Wuhan 430070,China)
Abstract:Porous glass powder with controlled pore size was prepared from the sodium borosilicate glass by heat treatment and subsequently acid leaching.Scanning electron microscopy(SEM) and Brunauer-Emmett-Teller(BET) analysis were used to investigate the surface morphology and the pore size distribution of the porous glass,respectively.Then a porous glass substrate with evenly distributed pore size(about 50nm) was prepared by adhering the porous glass powder with a Na2O-Al2O3-B2O3-based low melting glass.The effects of treating temperature,treating time and particle size on the adhesion were also studied.
Keywords:porous glass powder  heat-treatment  low melting glass  adhesion
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