| 气质联用法测定纺织品中多环芳烃(PAHs) |
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| 引用本文： | 茅文良,汪磊,陈海相,张克和,俞杭芳,俞旭霞. 气质联用法测定纺织品中多环芳烃(PAHs)[J]. 现代纺织技术, 2011, 19(5): 49-52 |
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| 作者姓名： | 茅文良 汪磊 陈海相 张克和 俞杭芳 俞旭霞 |
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| 作者单位： | 1. 浙江理工大学先进纺织材料与制备技术教育部重点实验室,杭州,310018
2. 国家羽绒制品质量监督检验中心（萧山）,杭州,311202 |
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| 基金项目： | 长江学者与创新团队发展计划项目 |
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| 摘 要： | 建立了超声提取气相色谱/质谱联用(GC/MS)测定纺织品中多环芳烃(PAHs)含量的分析方法,研究了提取溶剂、提取时间和温度对提取效率的影响,确定最佳提取条件。该方法应用于纺织品中PAHs的检测,16种PAHs的线性范围为0.05～4.0mg/L,方法检出限在0.012～0.094mg/kg内,加标回收率为68.7%～107.3%,相对标准偏差为0.58%～11.9%。方法简便可靠,能够达到纺织品中16种多环芳烃的检测要求。
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| 关 键 词： | 纺织品 多环芳烃 气相色谱/质谱 超声提取 测定 |
Determination of Polycyclic Aromatic Hydrocarbons in Textiles by GC/MS |
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| MAO Wenliang,WANG Lei,CHEN Haixiang,ZHANG Kehe,YU Hangfang,YU Xuxia,Hangzhou ,China). Determination of Polycyclic Aromatic Hydrocarbons in Textiles by GC/MS[J]. Advanced Textile Technology, 2011, 19(5): 49-52 |
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| Authors: | MAO Wenliang WANG Lei CHEN Haixiang ZHANG Kehe YU Hangfang YU Xuxia Hangzhou China) |
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| Affiliation: | MAO Wenliang1,WANG Lei1,CHEN Haixiang1,ZHANG Kehe1,YU Hangfang2,YU Xuxia2(1.The Key Laboratory of Advanced Textile Materials and Manufacturing Technology of the Ministry of Education,Zhejiang Sci-Tech University,Hangzhou 310018,China,2.China National Down & Feather Products Inspection and Testing Center(Xiaoshan),Hangzhou 311202,China) |
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| Abstract: | An analytical method for the determination of polycyclic aromatic hydrocarbons（PAHs） in textiles by supersonic extraction coupled with gas chromatography and mass spectrometry was developed.Through analyzing the effect of extraction solvent,extraction time and temperature on the extraction efficiency,the optimal extraction condition was confirmed.With this method to detect PHAs in textiles,the linearity range of 16 kinds of PHAs varied from 0.05mg/L to 4.0mg/L,the detection limits of this method ranged from 0.012mg/kg to 0.094mg/kg.The recovery rate was from 68.7% to 107.3% with the relative standard deviation ranging from 0.58% to 11.9%.The method was convenient and reliable,can meet the requirement of determination of 16 kinds of PHAs in textiles. |
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| Keywords: | textiles polycyclic aromatic hydrocarbons GC/MS supersonic extraction determination |
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