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国产ICP-AES测定润滑油中金属元素
引用本文:陈再洁,王智,李鹤,李小侠,徐以飞. 国产ICP-AES测定润滑油中金属元素[J]. 广州化工, 2010, 38(4): 129-131
作者姓名:陈再洁  王智  李鹤  李小侠  徐以飞
作者单位:江苏天瑞仪器股份有限公司,江苏,昆山,215300
摘    要:采用湿式消化法,利用国产江苏天瑞仪器的ICP-2000同时测定发动机用润滑油中痕量金属元素(Fe、P、Ca、Mg、Cu、Ni、Al等)。样品消化完全,快速,检出限低,RSD3%,回收率为97.0%~103.0%。

关 键 词:电感耦合等离子体发射光谱法  润滑油  湿式消化

Determination of Metals in Lubricating Oil with Domestic ICP-AES
CHEN Zai-jie,WANG Zhi,LI He,LI Xiao-xia,XU Yi-fei. Determination of Metals in Lubricating Oil with Domestic ICP-AES[J]. GuangZhou Chemical Industry and Technology, 2010, 38(4): 129-131
Authors:CHEN Zai-jie  WANG Zhi  LI He  LI Xiao-xia  XU Yi-fei
Affiliation:CHEN Zai -jie, WANG Zhi, LI He, LI Xiao - xia, XU Yi -fei (Skyray Instrument Co. , Ltd. Jiangsu Province, Jiangsu Kunshan 215300, China)
Abstract:Using homemade Jiangsu Skyray Instrument ICP- 2000, the engine lubricating oil of trace metals as Fe, P, Ca, Mg, Cu, Ni, Al, etc. , were determined simultaneously by wet digestion method. The sample digestion was complete, fast, low detection limit and RSD 〈 3% with recovery 97.0% - 103.0%.
Keywords:inductively coupled plasma atomic emission spectrometry  lubricants  wet digestion
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