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热处理温度对Fe_(83.5)B_(15)Cu_(1.5)合金结构及性能影响
引用本文:张家胜,王进,郑志刚,刘仲武,余红雅,陈燕凌,汪民.热处理温度对Fe_(83.5)B_(15)Cu_(1.5)合金结构及性能影响[J].磁性材料及器件,2015(2):6-9,20.
作者姓名:张家胜  王进  郑志刚  刘仲武  余红雅  陈燕凌  汪民
作者单位:1. 华南理工大学 材料科学与工程学院,广东广州,510640;2. 广州市德珑电子器件有限公司,广东广州,510000
基金项目:广东省教育部产学研结合项目(2013B0910000721);中央高校基本业务费重点项目
摘    要:通过熔体快淬法制备具有(200)取向α-Fe晶粒的Fe83.5B15Cu1.5非晶纳米晶合金,并重点研究了在制备过程中α-Fe晶粒的产生以及贴棍面和自由面对合金结构与磁性能的影响规律。研究表明,Fe83.5B15Cu1.5合金在熔体快淬之后具有大量(200)择优方向的α-Fe晶粒。晶化热处理之后,贴辊面的微观形貌主要是球形纳米颗粒,而自由面的微观形貌主要是长度为200~300nm的片状多孔结构。经过热处理(温度390℃,保温时间10min)之后可获得最佳磁性能为:饱和磁感应强度Bs=1.83T,矫顽力Hc=8.7A/m。本研究对Fe基非晶合金软磁材料的发展具有积极意义。

关 键 词:Fe83.5B15Cu1.5非晶纳米晶合金  熔体快淬  热处理  饱和磁感应强度  矫顽力

Effect of heat treatment on the microstructure and magnetic properties of Fe83.5B15Cu1.5 alloys
ZHANG Jia-sheng,WANG Jin,ZHENG Zhi-gang,LIU Zhong-wu,YU Hong-ya,CHEN Yan-ling,WANG Min.Effect of heat treatment on the microstructure and magnetic properties of Fe83.5B15Cu1.5 alloys[J].Journal of Magnetic Materials and Devices,2015(2):6-9,20.
Authors:ZHANG Jia-sheng  WANG Jin  ZHENG Zhi-gang  LIU Zhong-wu  YU Hong-ya  CHEN Yan-ling  WANG Min
Affiliation:ZHANG Jia-sheng;WANG Jin;ZHENG Zhi-gang;LIU Zhong-wu;YU Hong-ya;CHEN Yan-ling;WANG Min;School of Material Science and Engineering, South China University of Technology;Guangzhou Deloop Electronic Device Co, Ltd;
Abstract:Fe83.5B15Cu1.5 amorphous/nanocrystalline alloys with (200) orientedα-Fe nanoparticles were prepared by melt spinning. And the effects of the free and contact side on the microstructure and magnetic properties for Fe83.5B15Cu1.5 alloys were investigated. The results show that the Fe83.5B15Cu1.5 alloy contains a large amount of (200)-preferred α-Fe and exhibits optimal magnetic properties after annealing at 390℃ for 10 miniates. After heat treatment, the Fe83.5B15Cu1.5 alloy exhibits sphere nanoparticles on the contact side while flake porous microstructure on the free side. The optimal properties of maximum Bs of 1.83T and a low Hc of 8.7A/m were obtained for sample treated at 390℃ for 10 miniates. This research is of guidance for development of Fe-based amorphous/nanocrystalline soft magnetic materials.
Keywords:Fe83  5B15Cu1  5 amorphous/nanocrystalline alloys  melt spinning  heat treatment  saturation magnetic flux density  coercivity
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