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Preparation and characterization of jet-electrodeposited nanocrystalline nickel coatings
作者姓名:潘勇  江山  戴翠英  唐甜  周兆锋  周益舂
作者单位:[1]Faculty of Materials, Optoelectronic and Physics, Xiangtan University, Xiangtan 411105, China [2]Key Laboratory of Low Dimensional Materials and Application Technology, Ministry of Education, Xiangtan University, Xiangtan 411105, China
基金项目:Project(2005AA01210) supported by the Hi-tech Research and Development Program of China; Project( 10525211 ) supported by Fund for Prominent Young Scholars from the Organization of NNSF of China; Project(06C840) supported by Scientific Research Fund of Hunan Provincial Education Department, China
摘    要:Nanocrystalline nickel coatings were prepared by both direct current(DC) and pulse current(PC) jet-electrodeposition. The influences of current density and jet velocity on the surface morphology, microstructure and preferred orientation of the coatings obtained were investigated by SEM, TEM and XRD. It is found that the current density strongly affects the microstructure of the nickel coating. An increase of the DC current density results in a slight increase of the grain size and preferred orientation progressive evolution (i.e. from (111) to (200)), whereas an increase of the PC current density leads to a certain decrease of the grain size and preferred orientation change (i.e. from (111) to a strong (220)). Moreover, jet velocity shows no significant effect on the grain size and preferred orientation for the nanocrystalline coatings obtained in both DC and PC within the range of jet velocity studied.

关 键 词:纳米涂层  纳米晶镍涂层  喷射电镀  电流密度
收稿时间:2007-07-15
修稿时间:2007-09-10

Preparation and characterization of jet-electrodeposited nanocrystalline nickel coatings
PAN Yong, JIANG Shan, DAI Cui-ying.Preparation and characterization of jet-electrodeposited nanocrystalline nickel coatings[J].Transactions of Nonferrous Metals Society of China,2007,17(A02):770-775.
Authors:PAN Yong  JIANG Shan  DAI Cui-ying
Abstract:
Keywords:nanocrystalline nickel  jet-electro deposition  deposition current density  jet velocity
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