| 2-氨基-3-硝基-6-甲氧基吡啶的合成研究 |
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| 引用本文： | 刘田宇,阎峰,关瑾,樊凯奇.2-氨基-3-硝基-6-甲氧基吡啶的合成研究[J].当代化工,2009,38(5):450-452. |
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| 作者姓名： | 刘田宇 阎峰 关瑾 樊凯奇 |
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| 作者单位： | 沈阳化工学院应用化学专业,辽宁,沈阳,110142 |
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| 摘 要： | 以2,6-二氯吡啶为原料,通过硝化、氨化、甲氧化合成2-氨基-3-硝基-6-甲氧基吡啶,反应总收率60.6%,产物结构通过IR、1HNMR进行结构表征,证明结构正确。
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| 关 键 词： | 2-氨基-3-硝基-6-甲氧基吡啶 中间体 合成 |
Synthesis of 2-Amino-3-nitropyridine-6-methoxy |
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| LIU Tian-yu,YAN Feng,GUAN Jin,FAN Kai-qi.Synthesis of 2-Amino-3-nitropyridine-6-methoxy[J].Contemporary Chemical Industry,2009,38(5):450-452. |
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| Authors: | LIU Tian-yu YAN Feng GUAN Jin FAN Kai-qi |
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| Affiliation: | (Shenyang University of Chemical Technology, Liaoning Shenyang 110142, China) |
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| Abstract: | 2-amino-3-nitropyridine-6-methoxy was synthesized from 2,6- Dichloropyridine by substitution, nitration, ammoniation and oxidation. The overall yield of the reaction was 60.6%,the structure of the product was identified by IR and 1HNMR. The final product was gained. |
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| Keywords: | Amino-3-nitropyridine-6-methoxy Intermediate Synthesis |
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