| 杀螨杀菌剂二硝巴豆酸酯的合成 |
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| 引用本文： | 徐守林.杀螨杀菌剂二硝巴豆酸酯的合成[J].现代农药,2011,10(2):14-16. |
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| 作者姓名： | 徐守林 |
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| 作者单位： | 江苏快达农化股份有限公司,江苏如东,226401 |
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| 摘 要： | 报道了杀螨杀菌剂二硝巴豆酸酯的合成方法,由邻、对异辛基苯酚混合物为起始原料,经硝化反应后与由2-丁烯酸与光气合成的2-丁烯酰氯反应合成二硝巴豆酸酯,产品含量为92%～93%,产品总收率为79%(以邻、对异辛基苯酚混合物计),对各步反应工艺参数进行分析,得出最佳的合成工艺参数。
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| 关 键 词： | 杀螨杀菌剂 二硝巴豆酸酯 合成 |
Synthesis of Acaricidal Fungicide Dinocap |
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| XU Shou-lin.Synthesis of Acaricidal Fungicide Dinocap[J].Modern Agrochemicals,2011,10(2):14-16. |
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| Authors: | XU Shou-lin |
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| Affiliation: | XU Shou-lin(Jiangsu Kuaida Agrochemical Co.,Ltd.,Jiangsu Rudong 226401,China) |
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| Abstract: | Acaricidal fungicide dinocap was synthesized by using the mixture of o,p-isooctyl phenol as started material,that reacted with nitration and crotonyl chloride which was generated by reaction of crotonic acid and phosgene.Its' purity was 92%-93%,total yield was 79%(calculated as o,p-isooctyl phenol).The synthetic process of acaricidal fungicide dinocap was also been optimized. |
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| Keywords: | acaricidal fungicide dinocap synthetic process |
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