| 噻吩甲酰基二茂铁的合成及表征 |
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| 引用本文： | 郭书玲. 噻吩甲酰基二茂铁的合成及表征[J]. 广州化工, 2010, 38(8): 122-123 |
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| 作者姓名： | 郭书玲 |
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| 作者单位： | 河南工业大学,河南,郑州,450001 |
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| 基金项目： | 河南工业大学校科研基金资助课题 |
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| 摘 要： | 噻吩甲酸作为起始原料与亚硫酰氯反应生成噻吩甲酰氯;在无水氯化铝催化下,二茂铁与噻吩甲酰氯的傅-科反应合成了新化合物噻吩甲酰基二茂铁,测定了熔点,通过红外和核磁对其结构进行了表征。
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| 关 键 词： | 噻吩甲酰基二茂铁 二茂铁 噻吩甲酸 合成 表征 |
Synthesis and Structural Characterization of Thenoylferrocene |
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| GUO Shu-ling. Synthesis and Structural Characterization of Thenoylferrocene[J]. GuangZhou Chemical Industry and Technology, 2010, 38(8): 122-123 |
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| Authors: | GUO Shu-ling |
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| Affiliation: | GUO Shu-ling (Henan University of Technology,Henan Zhengzhou 450001,China) |
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| Abstract: | As initial material thiophene carboxylic acid reacting with thionyl chloride gave thenoyl chloride.Catalyzed by anhydrous aluminium chloride,the novel compound thenoylferrocene was synthesized by friedel-crafts acylation of ferrocene with thenoyl chloride.Melting point was determined,and the structure of thenoylferrocene was characterized by IR and 1H NMR spectra. |
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| Keywords: | thenoylferrocene ferrocene thiophene carboxylic acid synthesis characterization |
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