Separation of the methyl esters of oleic,linoleic, and linolenic acids by column chromatography using cation exchange resin containing silver ion |
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| Authors: | C. F. Wurster J. H. Copenhaver P. R. Shafer |
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| Affiliation: | (1) Department of Biological Sciences, Darmouth College, Hanover, New Hampshire;(2) Department of Chemistry, Dartmouth College, Hanover, New Hampshire |
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| Abstract: | By taking advantage of the tendency of silver ion to form complexes with unsaturated compounds, the methyl esters of oleic, linoleic, and linolenic acids have been cleanly separated in good yield by column chromatography. The silver ion was supported by means of a cation exchange resin; no silver was ever eluted from the column. Aqueous methanol, pure methanol, and ethanol saturated with butene-1 were employed as solvents. |
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