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毛细管气相色谱法测定丙烯酸树脂中残余单体
引用本文:王妍,李亚波,石基强,隋红英,张鑫塘. 毛细管气相色谱法测定丙烯酸树脂中残余单体[J]. 中国涂料, 2009, 24(7): 40-44
作者姓名:王妍  李亚波  石基强  隋红英  张鑫塘
作者单位:大连振邦氟涂料股份有限公司,辽宁大连,116036
摘    要:丙烯酸树脂用乙酸丁酯溶解,采用毛细管气相色谱法分离树脂中的残余单体及溶剂,然后用内标法及氢火焰离子化检测器(FID)测定各残余单体的含量。该方法分离效果好,灵敏度高,操作简单,准确可靠。

关 键 词:毛细管  气相色谱  残余单体  内标法

Determination of residual monomer in the acrylic resin by capillary gas chromatography
Wang Yan,Li Yabo,Shi Jiqiang,Sui Hongying,Zhang Xintang. Determination of residual monomer in the acrylic resin by capillary gas chromatography[J]. China Paint, 2009, 24(7): 40-44
Authors:Wang Yan  Li Yabo  Shi Jiqiang  Sui Hongying  Zhang Xintang
Affiliation:; (Dalian Zebon Fluorocarbon Coatings Co.,Ltd., Dalian 116036, Liaoning Province)
Abstract:The acrylic rein is dissolved in butyl acetate and residual monomer and solvent in resin are separated by capillary gas chromatography. Internal standard method and FID are used to determine the content of the residual monomer in resin. The methods ale of good separating effect, simple operation and accurate.
Keywords:capillary   chromatography   residual monomer   internal standard method
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