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液质联用分析测定苦荞黄酮
引用本文:徐宝才,肖刚,丁霄霖,李丹. 液质联用分析测定苦荞黄酮[J]. 食品科学, 2003, 24(6): 113-117
作者姓名:徐宝才  肖刚  丁霄霖  李丹
作者单位:江南大学食品学院
摘    要:本文采用RP-HPLC-DAD/MS在苦荞籽粒中发现了山奈酚;并对苦荞中的总黄酮和其中的四种主要黄酮醇:槲皮素-3-芸香糖葡萄糖苷(Ⅰ)、芦丁(Ⅱ)、山奈酚-3-芸香糖苷(Ⅲ)、槲皮素(IV)进行了定量。总黄酮含量为0.174%~4.614%,(I)、(II)、(III)、(IV)在壳、麸皮、外层粉、心粉、山西苦荞粉中的含量分别为0.0153%~0.0448%,0.0816%~4.1054%,0.0043%~0.1330%,0.0062%~0.5332%。

关 键 词:苦荞  黄酮  液质联用  
文章编号:1002-6630(2003)06-0113-05

RP-HPLC-DAD/MS Determination of Flavanoids in Fagopytum.tataricum
XU Bao-Cai,XIAO Gang,DING Xiao-Lin,LI Dan. RP-HPLC-DAD/MS Determination of Flavanoids in Fagopytum.tataricum[J]. Food Science, 2003, 24(6): 113-117
Authors:XU Bao-Cai  XIAO Gang  DING Xiao-Lin  LI Dan
Abstract:The flavanoids in Fagopyrum. tataricum seeds,from Sichuan province were studied. The types of flavanoids werequercitin-3-rutinoglucoglucoside, quercitin-3-rutinoglucoside,rutin, kmaepferol-3-rutinoside, quercitin, kmaepferol.The con-tents of flavanoids in hull, bran, outer flour, inner flour of Sichuan Fagopyrum. tataricum and flour of Sanxi Fagopyrum. tataricumwere 0.505%,4.614%,3.098%,0.174% and 0.944%, respectively, among which rutin was the major constituent.
Keywords:Fagopytum. tataricum  flavanoids  RP-HPLC MS DAD  
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