| 氰烯菌酯的合成方法改进 |
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| 引用本文： | 曹庆亮,周健,马海军. 氰烯菌酯的合成方法改进[J]. 现代农药, 2014, 0(6): 11-12 |
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| 作者姓名： | 曹庆亮 周健 马海军 |
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| 作者单位： | 江苏南方农药研究中心,南京210046 |
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| 基金项目： | 国家“十二·五”科技支撑计划（2011BAE06B01-11） |
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| 摘 要： | 以苯甲腈、氰乙酸乙酯等为起始原料,经加成、缩合反应2步合成氰烯菌酯。通过提纯,产品质量分数达到95.0%,总收率大于72%。改进后的方法与原方法相比,线路缩短,易于工业化生产。
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| 关 键 词： | 氰烯菌酯 合成 提纯 |
Improvement on Synthesis of Phenamacril |
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| CAO Qing-liang,ZHOU Jian,MA Hai-jun. Improvement on Synthesis of Phenamacril[J]. Modern Agrochemicals, 2014, 0(6): 11-12 |
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| Authors: | CAO Qing-liang ZHOU Jian MA Hai-jun |
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| Affiliation: | (Jiangsu Southern Pesticide Research Center, Nanjing 210046, China) |
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| Abstract: | A novel synthetic method was studied. Using benzonitrile, ethyl cyanoacetate as starting materials, phenamacril was obtained by addition and condensation reaction. The purity of the product was 95.0% and the total yield was more than 72%. Compared with the original synthetic method, the novel method was simple and could be used in industry. |
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| Keywords: | phenamacril synthesis purification |
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