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GO/PI复合纳米纤维的制备及其过滤性能研究
引用本文:杨文秀,刘冬冬,胡雪敏. GO/PI复合纳米纤维的制备及其过滤性能研究[J]. 上海纺织科技, 2020, 48(3): 26-28,45
作者姓名:杨文秀  刘冬冬  胡雪敏
作者单位:河北科技大学纺织服装学院,河北石家庄050000;河北科技大学纺织服装学院,河北石家庄050000;河北科技大学纺织服装学院,河北石家庄050000
基金项目:河北省高等学校科学技术研究基金项目(ZD2017231);大学生创新创业训练计划项目(2019191)。
摘    要:为制备高过滤效率、低过滤阻力的空气过滤材料,将氧化石墨烯纳米颗粒(GO)掺杂到聚酰亚胺(PI)纺丝溶液中,制备氧化石墨烯/聚酰亚胺(GO/PI)复合纳米纤维过滤材料。通过观察其形貌、过滤性能来确定最优纺丝工艺参数。结果表明:当PI质量分数为30%,GO质量分数为1%,纺丝电压为25 kV,接收距离为20 cm时,复合纳米薄膜的纤维形貌较好,过滤性能优良。与PI纯组分纳米纤维过滤材料相比,GO/PI复合纳米纤维过滤材料的过滤性能更好,制得GO/PI复合纳米纤维膜的平均孔径为1.8μm,过滤效率为99.68%,过滤阻力仅为85.35 Pa。

关 键 词:过滤材料  静电纺丝  工艺参数  氧化石墨烯  聚酰亚胺  过滤性能

Preparation and filtration properties of GO/PI composite nanofibers
YANG Wenxiu,LIU Dongdong,HU Xuemin. Preparation and filtration properties of GO/PI composite nanofibers[J]. Shanghai Textile Science & Technology, 2020, 48(3): 26-28,45
Authors:YANG Wenxiu  LIU Dongdong  HU Xuemin
Affiliation:(School of Textile and Garment,Hebei University of Science and Technology,Shijiazhuang 050000,Hebei,China)
Abstract:In order to prepare air filtration materials with high filtration efficiency and low filtration resistance,graphene oxide nanoparticles are doped into polyimide(PI)spinning solution to prepare graphene oxide/polyimide(GO/PI)composite nanofiber filtration materials.The optimum spinning parameters are determined by observing the nanofier morphology and test filtration performance.The results show that when PI concentration is 30%,GO concentration is 1%,spinning voltage is 25 kV,and receiving distance is 20 cm,composite nanofiber film fiber has the best morphology and excellent filtration performance.Compared with pure component PI nanofiber filtration materials,GO/PI composite nanofiber filtration materials have better filtration performance.The average pore diameter of GO/PI composite nanofiber membrane is 1.8μm,the filtration efficiency is 99.68%,and the filtration resistance is only 85.35 Pa.
Keywords:filter material  electrostatic spinning  processing parameter  graphene oxide  polyimide  filtration performance
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