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不同方法制备二甲醚合成催化剂的物相表征
引用本文:杨德辽,陈良才,刘建江,张中亚,焦玲玲,闫海珍. 不同方法制备二甲醚合成催化剂的物相表征[J]. 化学工业与工程技术, 2009, 30(2): 26-28
作者姓名:杨德辽  陈良才  刘建江  张中亚  焦玲玲  闫海珍
作者单位:1. 中国石油天然气股份有限公司,塔里木油田石化分公司,新疆,库尔勒,841000
2. 华中科技大学能,源与动力工程学院,湖北,武汉,430074
3. 中国石油天然气股份有限公司,塔里木油田塔西南化肥厂,新疆,泽普,844804
摘    要:采用共沉淀法、浸渍法、机械混合法、胶体沉淀法制备了成分相同的二甲醚合成催化剂,通过X射线衍射法和电镜扫描法对催化剂进行了表征。结果发现,4种制备方法中,浸渍法制备的催化剂物相效果最理想,各成分分散均匀,粒径较小,无结块、烧结现象。

关 键 词:二甲醚  催化剂  制备方法  表征

Characterization of DME synthesis catalysts prepared by different methods
Yang Deliao,Chen Liangcai,Liu Jianjiang,Zhang Zhongya,Jiao Lingling,Yan Haizhen. Characterization of DME synthesis catalysts prepared by different methods[J]. Journal of Chemical Industry & Engineering, 2009, 30(2): 26-28
Authors:Yang Deliao  Chen Liangcai  Liu Jianjiang  Zhang Zhongya  Jiao Lingling  Yan Haizhen
Affiliation:Yang Deliao ,Chen Liangcai , Liu Jianjiang , Zhang Zhongya , Jiao Lingling , Yan Haizhen (1. Petro China Tarim Oilfield Petrochemical Company, Korla 841000, China;2. Institute of energy & power, Huazhong University of Science and Technology,Wuhan 430074, China; 3. Fertilizer Plant of South-Western Tarim Exploration & Development Company, Petro China Tarim Oilfiled, Zepu 844804, China )
Abstract:Catalysts with the same composition for synthesis dimethyl ether are prepared by co-precipitation,impregnation,mechanical mixing,colloidal precipitation method.The catalyst is characterized by DEM and XRD.The rulsts show that the effects of catalyst prepared by impregnation are optimal in four methods: particles distribute in a steady uniform,crystal size is small,has no sintering phenomenon.
Keywords:Dimethyl ether  Catalyst  Preparation method  Characterization
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