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Bimodal plate structures induced by pulsed laser in duplex-phase Zr alloy
Authors:LinJiang Chai  ShuYan Wang  Hao Wu  ZhiNan Yang  HuCheng Pan  Bo Song  Ning Guo
Affiliation:1.College of Materials Science and Engineering,Chongqing University of Technology,Chongqing,China;2.National Engineering Research Center for Equipment and Technology of Cold Strip Rolling,Yanshan University,Qinhuangdao,China;3.Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education),Northeastern University,Shenyang,China;4.Faculty of Materials and Energy,Southwest University,Chongqing,China
Abstract:A duplex-phase Zr-2.5Nb alloy was treated by pulsed laser, followed by careful microstructural characterization using field emission gun scanning electron microscope and attached electron backscatter diffraction. Beneath the modification zones with common uniform α-plate structures (UPS), a layer of unreported bimodal α-plate structures (BPS) featured by coarse (submicron) plates forming multiple cores surrounded by dense fine (nanoscale) plates was found. Presence of such BPS is attributed to non-equilibrium thermodynamic conditions induced by the pulsed laser treatments. Limited diffusion of Nb due to the short pulse during laser heating allows β phases with distinctly different Nb contents to be presented: Nb-enriched prior β films and Nb-depleted β phases, transforming into the fine and the coarse plates during cooling, respectively. Orientation analyses show that both types of plates in the BPS are aroused essentially from a single β orientation, suggesting epitaxial growth of the Nb-depleted β phases from the preexisting β films.
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