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Synthesis and Preliminary Tests of Suspension Plasma Spraying of Fine Hydroxyapatite Powder
Authors:Roman Jaworski  Christel Pierlot  Lech Pawlowski  Muriel Bigan  Maxime Quivrin
Affiliation:1. Service of Thermal Spraying at Ecole Nationale Supérieure de Chimie de Lille, BP 90180, 8 avenue Mendele?ev, 59650, Villeneuve d’Ascq, France
2. LCOM, UMR CNRS 8009, ENSCL, BP 90108, F-59652, Villeneuve d’Ascq Cedex, France
Abstract:The synthetic hydroxyapatite (HA, Ca10(PO4)6(OH)2) is a very useful biomaterial for numerous applications in medicine, such as e.g., fine powder for suspension plasma spraying. The powder was synthesized using aqueous solution of ammonium phosphate (H2(PO4)NH4) and calcium nitrate (Ca(NO3) · 4H2O) in the carefully controlled experiments. The synthesized fine powder was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). The powder was formulated into water and alcohol based suspension and used to carry out the initial tests of plasma spraying onto titanium substrate. The phase analysis of sprayed coating was made with the XRD.
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