| 氯氟醚菊酯蚊香的气相色谱测定法 |
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| 引用本文： | 刘佳乐,张利萍,刘亚军. 氯氟醚菊酯蚊香的气相色谱测定法[J]. 广东化工, 2010, 37(5): 198-199 |
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| 作者姓名： | 刘佳乐 张利萍 刘亚军 |
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| 作者单位： | 广州立白企业集团有限公司,工程技术研发中心,广东,广州,510170 |
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| 基金项目： | 广州市番禺区科技攻关项目 |
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| 摘 要： | 文章采用气相色谱法分析盘式蚊香中氯氟醚菊酯的含量。用1∶1(体积比)甲醇-丙酮溶液作为溶剂,经超声波振荡器振荡2h后,以邻苯二甲酸二戊酯为内标,HP-5石英毛细柱分离,氢火焰离子化检测器(FID)检测。分析结果表明,氯氟醚菊酯的线性相关系数为0.9999,标准偏差为0.0026,变异系数为2.90%,回收率在98.93%～100.62%之间。
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| 关 键 词： | 氯氟醚菊酯 气相色谱 氢火焰离子化检测器 |
GC Analysis of Meperfluthrin Mosquito Coil |
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| Liu Jiale,Zhang Liping,Liu Yajun. GC Analysis of Meperfluthrin Mosquito Coil[J]. Guangdong Chemical Industry, 2010, 37(5): 198-199 |
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| Authors: | Liu Jiale Zhang Liping Liu Yajun |
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| Affiliation: | (R＆D Center, Guangzhou Liby Enterprise Group Co., Ltd., Guangzhou 510170, China) |
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| Abstract: | A GC-FID method was developed for determination of meperfluthrin with dipentyl phthalate as internal standard with. The sample used 1 ： 1 methanolacetone as solvent, was shaked for2h and separated with HP-5 capillary column, detected with FID. The result showed that the linear coefficient of meperfluthrin was 0.9999, the standard deviation was 0.0026, the coefficient of variation was 2.90 %, and the average recovery was between 98.93 % and 100.62 %. |
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| Keywords: | meperfluthrin GC FID |
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