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复合包覆SrAl_2O_4:Eu~(2+),Dy~(3+)发光粉的生产工艺
引用本文:喻胜飞,罗武生. 复合包覆SrAl_2O_4:Eu~(2+),Dy~(3+)发光粉的生产工艺[J]. 中国粉体技术, 2013, 19(3): 35-38
作者姓名:喻胜飞  罗武生
作者单位:1. 中南林业科技大学材料科学与工程学院,湖南长沙,410004
2. 中南林业科技大学机电工程学院,湖南长沙,410004
摘    要:以马来酸酐(MA)和吲哚啉螺苯并吡喃(SP)为原料,在SrAl2O4∶Eu2+,Dy3+(SAO-ED)发光粉的表面进行复合包覆制备MA-SP-SAO-ED复合发光粉,探讨MA与SP的质量比、MA和SP的加入顺序对复合发光粉性能的影响,并用扫描电镜表征复合发光粉的表面涂层。结果表明,当MA和SP同时加入SAO-ED二氯甲烷溶液中,总加入量为SAO-ED发光粉质量的10%,且MA与SP的质量比为6∶1时,复合发光粉具有较好的耐水、光致发光和光致变色等性能;在SAO-ED发光粉表面包覆了均匀致密涂层。

关 键 词:发光粉  表面包覆  耐水性

Technology of Composite Coating SrAl2O4: Eu2+, Dy3+ Phosphors
YU Shengfei , LUO Wusheng. Technology of Composite Coating SrAl2O4: Eu2+, Dy3+ Phosphors[J]. China Powder Science and Technology, 2013, 19(3): 35-38
Authors:YU Shengfei    LUO Wusheng
Affiliation:b(a.College of Material Science and Engineering;b.College of Mechanical and Electrical Engineering,Central South University of Forestry and Technology,Changsha 410004,China)
Abstract:MA-SP-SAO-ED composite phosphors were prepared with two organic materials maleic anhydride(MA) and indoline spiropyrans(SP) directly coated on the surface of SrAl2O4∶Eu2+,Dy3+(SAO-ED) phosphors.The effect of the mass ratio and adding order of MA and SP on the properties of MA-SP-SAO-ED composite phosphors was discussed.The coating of the composite phosphors was characterized by SEM.The results show that the coated SAO-ED phosphors have higher water resistance and photoluminescence and photochromic properties when the mass ratio of MA and SP is 6∶1 and the total mass fraction is 10%.A homogenous and compact coating layer is formed.
Keywords:phosphor  coating  water resistance
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