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Superplastic behavior of reciprocating extruded Mg-6Zn-1Y-0.6Ce-0.6Zr from rapidly solidified ribbons
Authors:Xuefeng Guo  Wenpeng Yang  Fang Ren
Affiliation:1. School of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo, 454000, China
2. School of Materials Science and Engineering, Xi??an University of Technology, Xi??an, 710048, China
3. School of Economics and Management, Henan Polytechnic University, Jiaozuo, 454000, China
Abstract:RRE-Mg66 alloy with a composition of Mg-6.0%Zn-1.0%Y-0.6%Ce-0.6Zr was prepared by combinatorial processes of rapid solidification, reciprocating extrusion and extrusion. Microstructure was evaluated on SEM and TEM. The average grain size of the alloy is 0.7 ??m, the size of the second phase at grain boundary is 0.15 ??m, and the size of the intragranular precipitates in round shape is less than 20 nm. Superplastic behavior of the material was investigated in a temperature range of 150 to 250 °C and initial strain rate range of 3.3×10?4 to 3.3×10?2 s?1 in air. The highest elongation of 270% was obtained at 250 °C and 3.3× 10?3 s?1. High-strain-rate superplasticity and low-temperature superplasticity were achieved. The superplasticity results from intragranular sliding (IGS) at temperatures from 170 to < 200 °C and grain boundaries sliding (GBS) at 250 °C. At 200 °C a combination of IGS and GBS contributes to the superplastic flow.
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