| 钛硅ZSM—5分子筛的合成与表征 |
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| 引用本文： | 刘云凌,杜红宾.钛硅ZSM—5分子筛的合成与表征[J].石油学报(石油加工),1996,12(4):26-29. |
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| 作者姓名： | 刘云凌 杜红宾 |
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| 作者单位： | 吉林大学化学系!长春130023 |
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| 基金项目： | 国家自然科学基金，吉林大学无机水热合成开放实验室资助项目 |
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| 摘 要： | 采用水热晶化法，利用比较廉价的正丁胺为模板剂合成出Ｔｉ－ＺＳＭ－５型分子筛，探讨了它的合成影响因素，利用ＸＲＤ、ＳＥＭ、ＩＲ等方法对Ｔｉ－ＺＳＭ－５分子筛的结构作了表片，结果表明钛已进入分子筛骨架。
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| 关 键 词： | ZSM－5 分子筛 合成 表征 钛 硅 |
SYNTHESIS OF TITANIUM SILICALITE-1 ZEOLITE BYUSING BUTYLAMINE AS THE TEMPLATE |
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| Liu Yunling Du Hongbin Zhou FengqiPang Wenqin.SYNTHESIS OF TITANIUM SILICALITE-1 ZEOLITE BYUSING BUTYLAMINE AS THE TEMPLATE[J].Acta Petrolei Sinica (Petroleum Processing Section),1996,12(4):26-29. |
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| Authors: | Liu Yunling Du Hongbin Zhou FengqiPang Wenqin |
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| Abstract: | Titanium silicalite-1 (Ti-ZSM-5) was synthesized by using the less expensive n-butylamine as the template. The influence of variables for synthesis parameters such as SiO2/TiO2, H2O/SiO2 and BuNH2/SiO2 on synthesis of Ti-ZSM-5 are discussed. The synthesizedtitanium ZSM-5 zeolites were characterized by means of XRD, SEM and IR methods. Therewere evidences that Ti was incorporated into the framework of ZSM-5 zeolite. |
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| Keywords: | Ti-ZSM-5 zeolite synthesis characterization |
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