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Rapid synthesis of thermally stable hydroxyapaptite |
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| Authors: | Rabia NazirNida Iqbal Abdul S. KhanAftab Akram Anila AsifAqif A. Chaudhry Ihtesham ur. RehmanRafaqat Hussain |
| Affiliation: | a Interdisciplinary Research Centre in Biomedical Materials, COMSATS Institute of Information Technology, Lahore, 56000, Pakistan b School of Chemical and Materials Engineering, National University of Sciences and Technology, H-12, Islamabad, Pakistan c The Kroto Research Institute, Department of Materials Science and Engineering, University of Sheffield, Sheffield, S3 7HQ, United Kingdom d Department of Chemistry, University Teknologi Malaysia, 81310 UTM Skudai, Johor Darul Ta’zim, Malaysia |
| Abstract: | We have optimized the wet precipitation synthesis of hydroxyapaptite to obtain thermally stable powder in the short time span of 3 min. Exposure of the reaction mixture to 1000 W microwave for 3 min furnished hydroxyapatite, which was thermally stable at temperatures up to 1200 °C. Powders were analyzed for phase purity using X-ray crystallography; chemical composition was studied using Fourier transform infrared spectroscopy while particle morphology was analyzed using scanning electron microscopy. |
| Keywords: | Microwave Rapid synthesis Hydroxyapatite Biomaterial |
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