Phase, microstructure, and oxidation resistance of yttrium silicates coatings prepared by a hydrothermal electrophoretic deposition process for C/C composites |
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Authors: | Liu Miao Huang Jianfeng Zhang Yutao Deng Fei Cao Liyun Wu Jianpeng |
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Affiliation: | (1) School of Materials Science and Engineering, Shaanxi University of Science and Technology, Xi’an, Shaanxi, 710021, People’s Republic of China |
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Abstract: | Oxidation-resistant yttrium silicates coatings for SiC precoated carbon/carbon composites were prepared by a novel hydrothermal
electrophoretic deposition process. Sonochemical-synthesized yttrium silicates nanocrystallites, isopropanol, and iodine were
respectively used as source materials, solvent, and charging agent during the deposition. Phase compositions, surface and
cross-section microstructures of the as-prepared multilayer coatings were characterized by an X-ray diffractometer (XRD) and
a scanning electron microscopy (SEM). The influence of deposition temperatures on the phase, microstructure, and oxidation
resistance of the multilayer coated C/C composites was particularly investigated. Results show that the as-prepared outer
coatings are composed of yttrium silicates crystallites with a main phase of Y2Si2O7 and Y2SiO5. The thickness and density of the yttrium silicates coatings are improved with the increase of deposition temperature. Compared
with SiC coating prepared by pack cementation, the multilayer coatings prepared by pack cementation with a later hydrothermal
electrophoretic deposition process exhibit better antioxidation properties. The as-prepared multilayer coatings can effectively
protect C/C composites from oxidation at 1773 K in air for 35 h with a weight loss of 0.32 × 10−3 g/cm2. |
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