| 微波消解-氢化物原子荧光法测定鱼油中铅 |
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| 引用本文： | 叶嘉荣,郭新东,罗海英,苏永祺,吴玉銮.微波消解-氢化物原子荧光法测定鱼油中铅[J].广州化工,2006,34(2):52-53. |
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| 作者姓名： | 叶嘉荣 郭新东 罗海英 苏永祺 吴玉銮 |
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| 作者单位： | 广州市产品质量监督检验所,广东,广州,510110;广州市产品质量监督检验所,广东,广州,510110;广州市产品质量监督检验所,广东,广州,510110;广州市产品质量监督检验所,广东,广州,510110;广州市产品质量监督检验所,广东,广州,510110 |
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| 摘 要： | 建立了一种微波消解样品、氢化物发生原子荧光法测定鱼油中的铅含量的方法。该方法在选定的操作条件下,测定鱼油中铅的回收率为94.8％～102.3％,最低检出限为0.45ng/mL,相对标准偏差为5.2％。本方法操作简单、快速、灵敏度高,用于测定鱼油中的铅,结果良好。
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| 关 键 词： | 鱼油 铅 微波消解 氢化物发生原子荧光法 |
Determination of Lead in Fish Oil by Microwave Digestion Hydride Generation-Atomic Fluorescence Spectrometry |
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| YE Jia-rong,GUO Xin-dong,LUO Hai-ying,SU Yong-qi,WU Yu-luan.Determination of Lead in Fish Oil by Microwave Digestion Hydride Generation-Atomic Fluorescence Spectrometry[J].GuangZhou Chemical Industry and Technology,2006,34(2):52-53. |
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| Authors: | YE Jia-rong GUO Xin-dong LUO Hai-ying SU Yong-qi WU Yu-luan |
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| Affiliation: | National Centre for Quality Supervision and Testing of Processed Food (Guangzhou |
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| Abstract: | A novel method of the determination of lead in fish oil by microwave digestion hydride generation atomic fluorescence spectrometry was found. The detection limit , recovery rate, and RSD were 0.45 ng/mL,94. 8 %-102.3 % , and 5.2 % respectively under selected condition . The method is simple, fast and accurate for the determination of lead in fish oil. |
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| Keywords: | fish oil lead microwave digestion hydride generation-atomic fluorescence spectrometry |
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