Determination of phosphorus in oils using oxygen bomb ashing |
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| Authors: | W. K. Yuen P. C. Kelly |
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| Affiliation: | (1) Research Centre, Canada Packers, Inc., 2211 St. Clair Avenue West, M6N 1K4 Toronto, Ontario, Canada;(2) Present address: Saskatchewan Research Council, 30 Campus: Drive, S7N OX1 Saskatoon, Sask., Canada |
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| Abstract: | A fast method for phosphorus determination in an oil matrix is described. The principle of the method is similar to that of the AOCS method, but the ashing of the oil is accelerated using an oxygen bomb. In addition, a rapid molybdovanadate reagent is used for colorimetry rather than the molybdenum blue reagents specified in the AOCS method. Agreement with the air ashing procedure averages less than 5% difference above 10 μg/g. The detection limit is in the order of 1~2 μg/g. |
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