| 液晶中间体4-(2,3-二氟-4-烷氧基)苯基环己醇的合成研究 |
| |
| 引用本文： | 武生喜,董兆恒,杨东杰,冯星. 液晶中间体4-(2,3-二氟-4-烷氧基)苯基环己醇的合成研究[J]. 应用化工, 2010, 39(9) |
| |
| 作者姓名： | 武生喜 董兆恒 杨东杰 冯星 |
| |
| 作者单位： | 西安瑞联近代电子材料有限责任公司,陕西,西安,710077 |
| |
| 基金项目： | 西安市重点技术创新项目 |
| |
| 摘 要： | 以4-(2,3-二氟-4-烷氧基)苯基环己醇甲酸酯为原料,在碱性条件下水解反应得到4-(2,3-二氟-4-烷氧基)苯基环己醇液晶中间体,经过重结晶得到合格的目的产品,GC含量>99.8%,收率>95%。目的产物通过了GC-MS,DSC,IR等的确认。
|
| 关 键 词： | 合成 水解 液晶 4-(2,3-二氟-4-烷氧基)苯基环己醇 |
Study on synthesis of liquid crystal intermediate 4-(2,3-difluorine-4-n-alkoxy) phenyl cyclohexanol |
| |
| WU Sheng-xi,DONG Zhao-heng,YANG Dong-jie,FENG Xing. Study on synthesis of liquid crystal intermediate 4-(2,3-difluorine-4-n-alkoxy) phenyl cyclohexanol[J]. Applied chemical industry, 2010, 39(9) |
| |
| Authors: | WU Sheng-xi DONG Zhao-heng YANG Dong-jie FENG Xing |
| |
| Abstract: | Using 4-(2,3-difluorine-4-n-alkoxy) phenyl cyclohexyl formate as raw material,on the condition of alkali,4-(2,3-difluorine-4-n-alkoxy) phenyl cyclohexanol was composed by hydrolysis reaction,after crystallization of qualified products,content of target product.GC is over 99.8%.Recovery is over 95% and the products were characterized by GC-MS,DSC,IR. |
| |
| Keywords: | synthesis hydrolysis liquid crystal 4-(2,3-difluorine-4-n-alkoxy) phenyl cyclohexanol |
| 本文献已被 万方数据 等数据库收录！ |
|
