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AFS测定锌精矿中汞含量的不确定度评定
引用本文:曾何华,赵秀峰,吕晓华,牟锟.AFS测定锌精矿中汞含量的不确定度评定[J].广东化工,2011,38(9):146-148.
作者姓名:曾何华  赵秀峰  吕晓华  牟锟
作者单位:1. 昌吉学院化学与应用化学系,新疆昌吉,831100
2. 阿拉山口出入境检验检疫局技术中心,新疆阿拉山口,833418
摘    要:对氢化物发生-冷原子荧光光谱法测定锌精矿中的汞含量的过程进行了分析。不确定度的主要来源主要为标准溶液的配制、样品称量、定容及重复测定。当锌精矿中汞含量为0.056%时,测量结果表示为0.056(1±0.0839)%。

关 键 词:原子荧光光谱法  不确定度  

Uncertainty of Determination of Mercury Content in Zinc Concentrate by AFS
Zeng Hehua,Zhao Xiufeng,Lv Xiaohua,Mu Kun.Uncertainty of Determination of Mercury Content in Zinc Concentrate by AFS[J].Guangdong Chemical Industry,2011,38(9):146-148.
Authors:Zeng Hehua  Zhao Xiufeng  Lv Xiaohua  Mu Kun
Affiliation:Zeng Hehua1,Zhao Xiufeng1,Lv Xiaohua2,Mu Kun2(1.Department of Chemistry & Applied Chemistry Changji University,Changji 831100,2.Technical Center,Alashankou Entry-Exit Inspection & Quarantine Bureau,Alashankou 833418,China)
Abstract:Through analysis the progress of determining mercury content zinc concentrate by hydride generation-cold atomic fluorescence spectrometry.The main uncertainty sources were the preparation of standard solution,the weighing process of sample,the constant volume of sample,and the repeatability of determination results.When mercury content in zinc concentrate was 0.056 %,the determination result was 0.056(1±0.0839)%.
Keywords:fluorescence spectrometry  uncertainty  mercury  
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