| 微波辐射下6-羟基-2-苯基-3-哒酮衍生物的合成 |
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| 引用本文： | 路玉锋,刘书睿,张景,王芳,张艳华,刘信刚.微波辐射下6-羟基-2-苯基-3-哒酮衍生物的合成[J].河北化工,2007,30(7):47-48,76. |
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| 作者姓名： | 路玉锋 刘书睿 张景 王芳 张艳华 刘信刚 |
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| 作者单位： | 1. 华北制药集团制剂有限公司,河北,石家庄,050011
2. 河北科技大学实业开发总公司,河北,石家庄,050018 |
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| 摘 要： | 讨论了在微波辐射作用下,以顺丁烯二酸酐与肼类进行缩合反应合成6-羟基-2-苯基-3-哒酮衍生物,与传统的方法相比,该方法的优点是反应速度显著提高,而且处理方法简便、快捷,产率较高(达到98%).
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| 关 键 词： | 微波辐射 缩合 顺丁烯二酸酐 肼 |
| 文章编号： | 1003-5095（2007）07-0047-03 |
| 修稿时间： | 2007-05-21 |
The Compound of 6-Hydroxide-2-phenyl-3-pyridazone Ramification in the Condition of Microwave Radiation |
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| LU Yu-feng,LIU Shu-rui,ZHANG Jing,WANG Fang,ZHANG Yan-hua,LIU Xin-gang.The Compound of 6-Hydroxide-2-phenyl-3-pyridazone Ramification in the Condition of Microwave Radiation[J].Hebei Chemical Engineering and Industry,2007,30(7):47-48,76. |
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| Authors: | LU Yu-feng LIU Shu-rui ZHANG Jing WANG Fang ZHANG Yan-hua LIU Xin-gang |
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| Affiliation: | 1. North China Pharmaceutical Grop Formulation Co. ,Ltd, Shijiazhuang,050011,China;2. Industry Develop. Company of Hebei University of Science and Technology, Shijiazhuang 050018, China |
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| Abstract: | We discussed that in the condition of microwave radiation,the polycondensation of maleic anhydride and hydrazine become pyridazone ramification, comparing with the traditional method,the advantage of it is that the speed of compound is quietly improved,and the method of handled is simple and fast, the yields is higher(attain 98%). |
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| Keywords: | microwave radiation polycondensation maleic anhydride hydrazine |
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