| 氯甲基三唑盐酸盐的合成 |
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| 引用本文： | 孙克 吕良忠. 氯甲基三唑盐酸盐的合成[J]. 农药, 1996, 35(10): 17-17 |
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| 作者姓名： | 孙克 吕良忠 |
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| 作者单位： | 沈阳化工研究院 |
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| 摘 要： | 本文介绍了三唑类农药中间体氯甲基三唑盐酸盐的合成方法，以１Ｈ－１，２，４－三唑，多聚甲醛为主要原料合成羟甲基三唑，再与氯化亚砜进行反应，合成氯甲基三唑盐酸盐，合成总收率为８９．２％。
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| 关 键 词： | 氯甲基三唑 羟甲基三唑 合成 中间体 农药 |
Synthesis of 1-(Chloromethyl) triazole Hydrochloride Salt |
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| Sun Ke,Liu Liangzhong. Synthesis of 1-(Chloromethyl) triazole Hydrochloride Salt[J]. Pesticides, 1996, 35(10): 17-17 |
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| Authors: | Sun Ke Liu Liangzhong |
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| Abstract: | H-1,2,4-Triazole was reacted with paraformaldehyde in the presence of catalyst to give hydroxymethyltriazole,which was further reacted with thionyl chloride to obtain chloromethyltriazole hydrochloride salt.Total yield was 89.2%,and the structure was confirmed by 1HNMR. |
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| Keywords: | hloromethyl)triazole synthesis. |
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