| 一步氧化法合成3-甲基-4-硝基苯酚工艺优化研究 |
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| 引用本文： | 谢平.一步氧化法合成3-甲基-4-硝基苯酚工艺优化研究[J].安徽化工,2010,36(5):21-24. |
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| 作者姓名： | 谢平 |
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| 作者单位： | 安徽华星化工股份有限公司,安徽,合肥,230088 |
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| 摘 要： | 以间甲基苯酚为基本原料,经过亚硝化、氧化反应合成了3-甲基-4-硝基苯酚,研究了一步氧化法合成的工艺参数,最终得到了一步氧化法合成3-甲基-4-硝基苯酚的较佳工艺条件。小试实验结果表明：在最佳工艺条件下,3-甲基-4-硝基苯酚的合成收率达到97%。
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| 关 键 词： | 3-甲基-4-硝基苯酚 间甲基苯酚 一步氧化法 合成工艺 |
Study on Synthetic of 3-Methyl-4-nitrophenol with One Step Oxidation |
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| XIE Ping.Study on Synthetic of 3-Methyl-4-nitrophenol with One Step Oxidation[J].Anhui Chemical Industry,2010,36(5):21-24. |
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| Authors: | XIE Ping |
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| Affiliation: | XIE Ping(Anhui Huaxing Chemical Industry Co.Ltd.,Hefei 230088,China) |
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| Abstract: | In this paper,the technological parameters of synthesis 3-methyl-4-nitrophenol were studied from 3 methylphenol reacting with nitrosation reaction and oxidation reaction.And the one step oxidation synthetic technological conditions were optimized.The results of small scale experiments proved that the yield was 97%. |
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| Keywords: | 3-methyl-4-nitrophenol 3-methylphenol one step oxidation synthetic synthetic technology |
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