| UPLC-MS/MS法测定美洛昔康中两个中间体杂质 |
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| 引用本文： | 孙桐,葛雪松,张新勇,卓静. UPLC-MS/MS法测定美洛昔康中两个中间体杂质[J]. 广州化工, 2022, 50(3): 85-88,105. DOI: 10.3969/j.issn.1001-9677.2022.03.028 |
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| 作者姓名： | 孙桐 葛雪松 张新勇 卓静 |
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| 作者单位： | 宿迁市食品药品检验所,江苏 宿迁 223800 |
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| 摘 要： | 建立UPLC-MS/MS法测定美洛昔康中杂质A和杂质B.采用ACQUITY UPLC?HSS T3 C18(2.1 mm×100 mm,1.8μm)色谱柱,流动相为0.1％甲酸水溶液-甲醇(45:55).采用电喷雾离子源(ESI),多反应监测(MRM)模式,正离子扫描;脱溶剂温度:500℃;干燥气流速:15 L/min...
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| 关 键 词： | 超高液相色谱质谱联用 美洛昔康 杂质A 杂质B 中间体 |
Determination of Two Intermediate Impuritiesin Meloxicam by UPLC-MS/MS |
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| SUN Tong,GE Xue-song,ZHANG Xin-yong,ZHUO Jing. Determination of Two Intermediate Impuritiesin Meloxicam by UPLC-MS/MS[J]. GuangZhou Chemical Industry and Technology, 2022, 50(3): 85-88,105. DOI: 10.3969/j.issn.1001-9677.2022.03.028 |
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| Authors: | SUN Tong GE Xue-song ZHANG Xin-yong ZHUO Jing |
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