An oscillatory pressure sintering of zirconia powder: Densification trajectories and mechanical properties |
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| Authors: | Yao Han Shuang Li Tianbin Zhu Weiwei Wu Di An Feng Hu Zunlan Hu Jian Liu Jingkun Xu Zhipeng Xie |
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| Affiliation: | 1. State Key Laboratory of New Ceramics and Fine Processing, School of Materials Science and Engineering, Tsinghua University, Beijing, China;2. School of Resources and Environmental Engineering, Shandong University of Technology, Zibo, China |
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| Abstract: | The densification trajectories and mechanical properties of zirconia ceramics obtained by oscillatory pressure sintering (OPS) process were investigated, during the sintering process an oscillatory pressure was applied at three stages. Current results indicated that at intermediate stage the oscillatory pressure revealed a favorable improvement of mechanical properties compared with conventional hot pressing (HP) and pressureless sintering (PS) procedures, while the enhancement was not obvious at initial stage. When the oscillatory pressure was applied at final stage, the OPS specimens exhibited the highest bending strength and hardness of 1455 ± 99MPa and 16.6 ± 0.31GPa compared with the PS and HP specimens. Considering the high elastic modulus and Moiré patterns observed in the OPS specimen, the oscillatory pressure applied at intermediate and final stages was detected to facilitate the sliding of grain boundary, plastic deformation of monolithic grains, the removal of pores and the strengthening of atomic bonds. |
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| Keywords: | mechanical properties oscillatory pressure sintering sintering stages zirconia ceramics |
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