Reduction of tungsten oxide to tungsten metal |
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Authors: | Theodore R Wilken William R Morcom Charles A Wert John B Woodhouse |
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Affiliation: | (1) Department of Metallurgy and Mining Engineering, University of Illinois, 61801 Urbana, IL;(2) Materials Research Laboratory, University of Illinois, 61801 Urbana, IL;(3) Westinghouse Lamp Divisions, 07003 Bloomfield, NJ |
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Abstract: | Tungsten oxide, WO2.96, was reduced toα-W in hydrogen for various time periods over the temperature range 500°C to 900°C. Intermediate oxides were determined using
X-ray diffraction analysis of the semireduced powders. Several dopant conditions were used, to find the effect on oxide structures
and reaction kinetics of the usual dopants K, Si and Al. The scanning electron microscope was employed to determine the morphology
of the crystallites at intermediate and final stages of reduction.
This research was supported in part by the U.S. Energy Research and Development Administration, Contract E(11-1)-1198. |
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