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纳米钨粉体的表征及其晶格畸变分析
引用本文:宋志华,郭亨群,张春华,王国立,吴冲浒,吴其山,吴志军.纳米钨粉体的表征及其晶格畸变分析[J].材料导报,2009,23(10).
作者姓名:宋志华  郭亨群  张春华  王国立  吴冲浒  吴其山  吴志军
作者单位:1. 华侨大学信息科学与工程学院,泉州,362021
2. 厦门金鹭特种合金有限公司,厦门,361006
基金项目:国家科技支撑计划,华侨大学科研启动项目 
摘    要:以工业化生产技术成功地制备了不同粒径的纳米W粉体,采用EDS、SEM和XRD对样品的含量、形貌、物相进行了表征,并计算了其晶格参数和晶胞体积.结果表明,纳米W粉体为bcc晶态结构,晶格发生收缩;随着晶粒尺寸的减小,晶格参数和晶胞体积收缩率增大,且晶格畸变率与粒径的倒数呈正比线性关系.

关 键 词:纳米钨粉  晶粒尺寸  晶格参数  晶格畸变

Characterization of Nano-tungsten Powder and Its Lattice Distortion Analysis
SONG Zhihua,GUO Hengqun,ZHANG Chunhua,WANG Guoli,WU Chonghu,WU Qishan,WU Zhijun.Characterization of Nano-tungsten Powder and Its Lattice Distortion Analysis[J].Materials Review,2009,23(10).
Authors:SONG Zhihua  GUO Hengqun  ZHANG Chunhua  WANG Guoli  WU Chonghu  WU Qishan  WU Zhijun
Affiliation:SONG Zhihua1,GUO Hengqun1,ZHANG Chunhua1,WANG Guoli1,WU Chonghu2,WU Qishan2,WU Zhijun1(1 College of Information Science , Engineering,Huaqiao University,Quanzhou 362021,2 Xiamen Golden Egret Special Alloy Co.Ltd,Xiamen 361006)
Abstract:Nano-W powder with various grain sizes are successfully produced on the basis of industrialized production technology.The content,morphology and phase of the samples are characterized by using EDS,SEM and XRD,and the lattice parameters and cell volume are worked out.The results indicate that nano-W powder have bcc crystal structure,the shrinkage of lattice has taken place.With the decrease of the grain sizes,the shrinkage rate of the lattice parameters and cell volume increases and the lattice distortion ra...
Keywords:nano-tungsten powder  grain size  lattice parameters  lattice distortion  
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