| 无溶剂微波催化合成1-(3-硝基苯基)-2-乙酰基丙烯酸酯 |
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| 引用本文： | 王向前,郭彦春. 无溶剂微波催化合成1-(3-硝基苯基)-2-乙酰基丙烯酸酯[J]. 河南化工, 2006, 23(4): 31-32 |
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| 作者姓名： | 王向前 郭彦春 |
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| 作者单位： | 郑州大学,化学系,河南,郑州,450052 |
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| 摘 要： | 微波无溶剂条件下,3-硝基苯甲醛和乙酰乙酸酯进行缩合反应,反应时间较传统方法大大缩短,而且收率达到或超过了传统方法.
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| 关 键 词： | 缩合 乙酰乙酸乙酯 微波 |
| 文章编号： | 1003-3467（2006）04-0031-02 |
| 收稿时间： | 2006-01-25 |
| 修稿时间： | 2006-01-25 |
Synthesis of 1-(3-Nitrophenyl)-2-acetyl-acrylic Ester under Microwave Irradiation without Solvent |
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| WANG Xiang-qian,GUO Yan-chun. Synthesis of 1-(3-Nitrophenyl)-2-acetyl-acrylic Ester under Microwave Irradiation without Solvent[J]. Henan Chemical Industry, 2006, 23(4): 31-32 |
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| Authors: | WANG Xiang-qian GUO Yan-chun |
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| Affiliation: | Department of Chemistry , Zhengzhou University , Zhengzhou 450052 , China |
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| Abstract: | Under microwave irradiation without solvent, the condensation of 3 - nitrobenzaldehyde and acetoacetic ester took place in much shorter time than conventional ways. The yield approach or exceed those of conventional ways. |
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| Keywords: | condensation acetoacetic ester microwave |
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