| 2(5H)-呋喃酮的过氧化氢氧化法合成与表征 |
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| 引用本文： | 郑绿茵,汪朝阳,李雄武,梁志群,陈秋妹,王少玲.2(5H)-呋喃酮的过氧化氢氧化法合成与表征[J].化学试剂,2005,27(12):751-752,754. |
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| 作者姓名： | 郑绿茵 汪朝阳 李雄武 梁志群 陈秋妹 王少玲 |
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| 作者单位： | 华南师范大学,化学与环境学院化学系,广东,广州,510631;华南师范大学,化学与环境学院化学系,广东,广州,510631;华南师范大学,化学与环境学院化学系,广东,广州,510631;华南师范大学,化学与环境学院化学系,广东,广州,510631;华南师范大学,化学与环境学院化学系,广东,广州,510631;华南师范大学,化学与环境学院化学系,广东,广州,510631 |
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| 摘 要： | 用过氧化氢氧化糠醛法合成2（5H）-呋喃酮,详细讨论了投料比例、反应温度、滴加方式、反应时间等对产率的影响,产物用FT-IR、UV、^1HNMR、MS等进行了表征.
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| 关 键 词： | 2(5H)-呋喃酮 过氧化氢 糠醛 合成 表征 |
| 文章编号： | 0258-3283（2005）12-0751-02 |
| 收稿时间： | 2005-04-21 |
| 修稿时间： | 2005-04-21 |
Synthesis of 2 (5H)-furanone by oxidation of furfural with hydrogen peroxide and its characterization |
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| ZHENG Lv-yin,WANG Zhao-yang,LI Xiong-wu,LIANG Zhi-qun,CHEN Qiu-mei,WANG Shao-ling.Synthesis of 2 (5H)-furanone by oxidation of furfural with hydrogen peroxide and its characterization[J].Chemical Reagents,2005,27(12):751-752,754. |
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| Authors: | ZHENG Lv-yin WANG Zhao-yang LI Xiong-wu LIANG Zhi-qun CHEN Qiu-mei WANG Shao-ling |
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| Affiliation: | Department of Chemistry, College of Chemistry and Environment, South China Normal University, Guangzhou 510631, China |
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| Abstract: | 2(5H)-Furanone was synthesized by oxidation of furfural with hydrogen peroxide.The influences of reaction conditions including dropping proportion of hydrogen peroxide and furfural,reaction temperature,dropping methods of hydrogen peroxide and reaction time on yield were discussed in detail.The structure of 2(5H)-furanone was characterized with FTIR,UV, 1HNMR and MS. |
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| Keywords: | 2(5H)-furanone hydrogen peroxide furfural synthesis characterization |
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