| 10-氨基十一酸合成工艺的研究 |
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| 引用本文： | 郝永莉,胡国胜. 10-氨基十一酸合成工艺的研究[J]. 河南化工, 2004, 0(2): 23-24 |
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| 作者姓名： | 郝永莉 胡国胜 |
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| 作者单位： | 华北工学院,高分子研究所,山西,太原,030051;华北工学院,高分子研究所,山西,太原,030051 |
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| 摘 要： | 以尼龙11单体生产中的副产品10-溴代十一酸为原料合成了10-氨基十一酸。由IR和^1H NMR确定了产物的结构。考察了反应时间、反应温度、原料配比、氨水浓度、蒸氨工艺条件等因素对产率的影响：优化了合成10-氨基十一酸的工艺条件。
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| 关 键 词： | 10-氨基十一酸 10-溴代十一酸 合成 |
| 文章编号： | 1003-3467(2004)02-0023-02 |
Study on Synthetic Process of 10-Aminoundecanoic Acid |
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| HAO Yong-li,HU Guo-sheng. Study on Synthetic Process of 10-Aminoundecanoic Acid[J]. Henan Chemical Industry, 2004, 0(2): 23-24 |
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| Authors: | HAO Yong-li HU Guo-sheng |
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| Abstract: | 10-Aminoundecanic acid is synthesized with 10-bromoundecanoic acid,a by-product in the production of nylon 11,as raw material. The structure of the product is characterized by IR and~1H NMR. The effects of reaction time, reaction temperature, molar ratio of materials, concentration of ammonia water, process conditions of evaporation of ammonia etc. on the yield of the product are investigated. The optimal conditions of process is obtained. |
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| Keywords: | 10-aminoundecanoic acid 10-bromoundecanoic acid synthesis |
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